[1] Huang Kuojun, GC - MS Analysis of Volatile Components in Curcuma Zedoary [J]. Journal of Shaanxi University of Traditional Chinese Medicine, 2020, (01): 69-75. [doi: 10.13424/j.cnki.jsctcm.2020.01.018]
GC - MS Analysis of Volatile Components in Curcuma Zedoary
- Article number:
- 2096-1340(2020)01-0069-07
- Keywords:
- curcuma zedoaria; volatile oil; GC - MS; qualitative analysis; quality control
- ZTFLH:
- R277
- Code:
- A
- Abstract:
- Objective To analyze the volatile components of curcuma zedoaria and explore the main components of the volatile oil. Methods Qualitative analysis was performed by GC - MS with Agilent 19091S - 433: 93. 92873 HP - 5MS 5% Phenyl Methyl silox -60 ℃ -325 ℃ ( 325 ℃) ( 0. 25μm × 0. 25 mm × 30 m) column; program temperature increase: initial temperature was 68 ℃, holding for 3 min, then increased to 160 ℃ at 5 ℃ / min, 220 ℃ at 7 ℃ / min,holding for 15 min; the carrier gas flow was 2. 0 mL/ min; split injection: injection Inlet temperature was 250 ℃, injection volume was 1 μL; the carrier gas for GC - MS is high purity helium ( ≥ 99. 999%) , the mass spectrum is EI source, the bombardment voltage is 70ev, the positive ion mode, the mass scanning range is 50 -550 amu, and the ion source temperature is 230 ℃. Results after analyzing 5 batches of curcuma zedoaria volatile oil samples, 44 components were identified. Conclusion The composition of volatile oil is complicated. The main components are ketene, olefin, and aromatic hydrocarbons. Among them, the content of epicurzereonoe, , curdione, germacrone, curzerene, β - elemene are abundant, which can provide scientific basis for the quality control research of curcuma zedoaria volatile oil and its related preparations.
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Memo
基金项目：湖北省食品药品监督检验研究院《湖北省中药材质量标准》《湖北省中药饮片炮制规范》新版编写项目 （鄂食药监办文［２０１５］２８号）