[1]朱晨曦 刘西京 林素静
** 王祥培.气质联用测定苦苣菜属三种植物的挥发油成分[J].陕西中医药大学学报,2018,(03):065-70.[doi:10.13424/j.cnki.jsctcm.2018.03.022]
Zhu Chenxi,Liu Xijing,Lin Sujing,et al.Determination of Volatile Oil Components in Three Species of Sonchus by GC - MS[J].Journal of Shaanxi University of Traditional Chinese Medicine,2018,(03):065-70.[doi:10.13424/j.cnki.jsctcm.2018.03.022]
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气质联用测定苦苣菜属三种植物的挥发油成分()
《陕西中医药大学学报》[ISSN:2096-1340/CN:61-1501/R]
- 卷:
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- 期数:
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2018年03期
- 页码:
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065-70
- 栏目:
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临床研究
- 出版日期:
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2018-05-10
文章信息/Info
- Title:
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Determination of Volatile Oil Components in Three Species of Sonchus by GC - MS
- 文章编号:
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2096-1340(2018)03-0065-07
- 作者:
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朱晨曦1; 2 刘西京2 林素静2
** 王祥培1
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1. 贵阳中医学院,贵州 贵阳 550000 ; 2. 深圳职业技术学院应用化学与生物技术学院,广东 深圳 518000
- Author(s):
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Zhu Chenxi1; 2; Liu Xijing2; Lin Sujing2; Wang Xiangpei1
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1. Guiyang University of Chinese Medicine,Guiyang 550000,China; 2. School of Applied Chemistry and Biotechnology in Shenzhen Polytechnic,Shenzhen 518000,China
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- 关键词:
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苣荬菜; 长裂苦苣菜; 花叶滇苦菜; 挥发油; 气相色谱—质谱联用
- Keywords:
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To analyze and compare the volatile oil components in endive; sonchus brachyotus and son- chus asper. Method: volatile oils of endive; sonchus brachyotus and sonchus asper were extracted by steam distillation and their chemical constituents were identified
- 分类号:
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R284
- DOI:
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10.13424/j.cnki.jsctcm.2018.03.022
- 文献标志码:
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A
- 摘要:
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目的 对苣荬菜、长裂苦苣菜、花叶滇苦菜中的挥发油成分进行分析与比较。方法 用水蒸气蒸馏法分别
提取苣荬菜、长裂苦苣菜、花叶滇苦菜的挥发油,采用气相色谱 -质谱联用法,鉴定其挥发油的化学成分。结果 苣荬菜
鉴定出35 种成分,长裂苦苣菜鉴定出55 种成分,花叶滇苦菜鉴定出 49 种成分。结论 苣荬菜的主要成分为 6,10,14 - 三甲基 -十五烷 -2 -酮( 26. 46%) 、植醇( 9. 67%) ,长裂苦苣菜的主要成分为正十六烷酸( 8. 01%) 、4 - ( 2,6,6 -三
甲基 -1 -环己烯 -1 -基) -3 -丁烯 -2 -酮( 7. 09%) ,花叶滇苦菜的主要成分为正十六烷酸( 12. 87%) 、6,10,14 -
三甲基 -十五烷 -2 -酮( 12%) 。三者共同的成分有6,10,14 -三甲基 -十五烷 -2 -酮、1,1,5 -三甲基 -1,2 -二
氢萘、( E) -1 - ( 2,6,6 -三甲基 -1,3 -环己二烯 -1 -基) -2 -丁烯 -1 -酮等11 种。
- Abstract:
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To analyze and compare the volatile oil components in endive,sonchus brachyotus and son- chus asper. Method: volatile oils of endive,sonchus brachyotus and sonchus asper were extracted by steam distillation and their chemical constituents were identified by GC - MS. Result: 35 components were identified from endive,55 com- ponents were identified from sonchus brachyotus,49 components were identified from sonchus asper. Conclusion: The main components of endive are 6,10,14 - trimethyl - pentadecan - 2 - ketone ( 26. 46% ) and phytol ( 9. 67% ) . The main components of sonchus brachyotus are n - hexadecanoic acid ( 8. 01% ) and 4 - ( 2,6,6 - trimethyl - 1 - cyclohex- ene - 1 - yl) - 3 - butene - 2 - ketone ( 7. 09% ) . The main components of sonchus asper are n - hexadecanoic acid ( 12. 87% ) and 6,10,14 - trimethyl - pentadecan - 2 - ketone ( 12% ) . The common components of the three are 6,10, 14 - trimethyl - pentadecan - 2 - ketone,1,1,5 - trimethyl - 1,2 - dihydronaphtha,( E) - 1 - ( 2,6,6 - trimethyl - 1 - cyclohexene - 1 - yl) - 2 - butene - 1 - ketone and other 8 species. To analyze and compare the volatile oil components in endive,sonchus brachyotus and son- chus asper. Method: volatile oils of endive,sonchus brachyotus and sonchus asper were extracted by steam distillation and their chemical constituents were identified by GC - MS. Result: 35 components were identified from endive,55 com- ponents were identified from sonchus brachyotus,49 components were identified from sonchus asper. Conclusion: The main components of endive are 6,10,14 - trimethyl - pentadecan - 2 - ketone ( 26. 46% ) and phytol ( 9. 67% ) . The main components of sonchus brachyotus are n - hexadecanoic acid ( 8. 01% ) and 4 - ( 2,6,6 - trimethyl - 1 - cyclohex- ene - 1 - yl) - 3 - butene - 2 - ketone ( 7. 09% ) . The main components of sonchus asper are n - hexadecanoic acid ( 12. 87% ) and 6,10,14 - trimethyl - pentadecan - 2 - ketone ( 12% ) . The common components of the three are 6,10, 14 - trimethyl - pentadecan - 2 - ketone,1,1,5 - trimethyl - 1,2 - dihydronaphtha,( E) - 1 - ( 2,6,6 - trimethyl - 1 - cyclohexene - 1 - yl) - 2 - butene - 1 - ketone and other 8 species. Keywords endive,sonchus brachyotus,sonchus asper,volatile oil,GC - MS
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备注/Memo
- 备注/Memo:
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基金项目: 深圳市科创委 2015 年基础研究项目( JCYJ2015 0630 1141 40632)
通讯作者: 林素静( 1977 - ) ,女,硕士,副教授,主要研究方向: 中药质量控制研究、药物制剂。E - mail: linsujing@ sz- pt. edu. cn. 收稿日期: 2017 - 09 - 28 编辑: 文颖娟
更新日期/Last Update:
2019-12-10